HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Phenanthro[1,2-b]furan-2-methanol → Phenanthro[1,2-b]thiophene-2-methanol
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Phenanthro[1,2-b]furan-2-methanol | HCID 14770239 | — |
| Edukt | Ethyl phenanthro[1,2-b]thiophene-2-carboxylate | HCID 14770247 | — |
| Lösungsmittel | Methylenechloride Hexane | HCID 21226440 | — |
| Produkt | Phenanthro[1,2-b]thiophene-2-methanol | HCID 14770248 | 98% |
Reaktionsschritte
Using the procedure outlined in 14A, ethyl phenanthro[1,2-b]thiophene-2-carboxylate (H. G. Pars Pharmaceutical Laboratories, Inc.) gave a 98.0% yield of phenanthro[1,2-b]thiophene-2-methanol, mp 169°-170.5° (C,H,S), (CH2Cl2 /hexane).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04910218 |
| Quelldatensatz | uspto-grants-1990_03 |
| ORD ID | ord-2a1c082b498f4072a07fea4c39a86b8e |
| Quellennotiz | uspto-grants-1990_03 |