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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1165656Generated: October 30, 2026

(+-)(2R*,3S*)-2-Methyl-2-nitro-1,3-butanediol → (+-)(2R*,3S*)-2-amino-2-methyl-1,3-butanediol acetate

https://huagongshe.com/reaction/1165656

Reaction equation

Participants

RoleNameHCIDCharge
Reactant(+-)(2R*,3S*)-2-Methyl-2-nitro-1,3-butanediolHCID 13375424—
Reactant(+-)(2R*,3R*)-2-amino-2-methyl-1,3-butanediol acetateHCID 86741969—
Product(+-)(2R*,3S*)-2-amino-2-methyl-1,3-butanediol acetateHCID 8674196693.5%

Reaction Steps

Using the procedure described for 32E, (±)-(2R*,3S*)-2-methyl-2-nitro-1,3-butanediol (32A, 41.1 g, 0.276 mol) gave 46.12 g (93.5%) of (±)-(2R*,3S*)-2-amino-2-methyl-1,3-butanediol acetate, mp 163°-165°, (C,H,N).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04910218
Source datasetuspto-grants-1990_03
ORD IDord-0b524eeb12634aeba618abb4f1525afa
Source noteuspto-grants-1990_03