Hexane → HCID 20065879, compound

HRID 1165658Notes

Reaction equation

HRID 1165658 reaction equation
[CH3:1][C:2]1[C:14]2[NH:13][C:12]3[CH:11]=[CH:10][C:9]4[CH:15]=[CH:16][CH:17]=[CH:18][C:8]=4[C:7]=3[C:6]=2[CH:5]=[CH:4][CH:3]=1.[CH3:19][CH2:20]CCCC>>[CH2:19]([N:13]1[C:12]2[CH:11]=[CH:10][C:9]3[CH:15]=[CH:16][CH:17]=[CH:18][C:8]=3[C:7]=2[C:6]2[CH:5]=[CH:4][CH:3]=[C:2]([CH3:1])[C:14]1=2)[CH3:20]

Participants

3

Reactant 2

HCID 8058HexaneHCID 20065887HCID 20065887, compound

Product 1

HCID 20065879HCID 20065879, compoundYield 79.1%

Procedure

Using the procedure outlined in Example 34A, 8-methyl-7H-benzo[c]carbazole (Cambridge Chemicals, Inc.) gave a 79.1% yield of 7-ethyl-8-methyl-7H-benzo[c]carbazole, mp 79°-83°, (hexane), (C,H,N).

Sources & evidence

ORD record
ord-cd70cf2d104b4817be19eebe35338b89
Source dataset
uspto-grants-1990_03
Patent number
US04910218

Reaction notes

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