Acetic acid, 2-isothiocyanato-, ethyl ester → HCID 14838133, compound

HRID 1165780Notes

Reaction equation

HRID 1165780 reaction equation
[CH2:1]([O:3][C:4]([CH2:6][N:7]=[C:8]=[S:9])=[O:5])[CH3:2].[CH2:10]([N:14]1[C:19]([NH:20][NH2:21])=[CH:18][C:17](=[O:22])[N:16]([CH2:23][CH2:24][CH3:25])[C:15]1=[O:26])[CH2:11][CH2:12][CH3:13]>O1CCOCC1>[CH2:10]([N:14]1[C:19]([NH:20][NH:21][C:8]([NH:7][CH2:6][C:4]([O:3][CH2:1][CH3:2])=[O:5])=[S:9])=[CH:18][C:17](=[O:22])[N:16]([CH2:23][CH2:24][CH3:25])[C:15]1=[O:26])[CH2:11][CH2:12][CH3:13]

Participants

4

Reactant 2

HCID 32202Acetic acid, 2-isothiocyanato-, ethyl esterHCID 13824276HCID 13824276, compound

Product 1

HCID 14838133HCID 14838133, compound

Reagents, catalysts & solvents 1

HCID 312751,4-DioxaneSolvent

Procedure

Ethoxycarbonylmethylisothiocyanate (15 g) was added dropwise to a stirred solution of 1-butyl-6-hydrazino-3-propylpyrimidine-2,4(1H,3H)-dione (11 g) in dioxane (100 ml).

Sources & evidence

ORD record
ord-a047722bdaf84b528b0c12c32fe975ae
Source dataset
uspto-grants-1990_03
Patent number
US04912104

Reaction notes

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