HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanol → HCID 18638369, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanol | HCID 887 | — |
| Reactant | HCID 4711769 | HCID 4711769 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Product | HCID 18638369 | HCID 18638369 | 95% |
Reaction Steps
Methyl α-benzoylamino-3,4-dimethoxycinnamate (20 g) was treated with 10% palladium on carbon (2 g) in methanol (400 mL) under a hydrogen atmosphere (1 atm.) for 3 days. The reaction mixture was then filtered and the solvent stripped to yield the title compound (18.90 g, 95%); MP 106°-107° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04912221 |
| Source dataset | uspto-grants-1990_03 |
| ORD ID | ord-2ab456710eba42ff8b970478179bc799 |
| Source note | uspto-grants-1990_03 |