HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl iodide → 2,6-Dichloro-4-nitroanisole
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl iodide | HCID 6328 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 2,4-Dichloro-6-nitrophenol | HCID 11871 | — |
| Product | 2,6-Dichloro-4-nitroanisole | HCID 169862 | 90.1% |
Reaction Steps
2-Nitro-4,6-dichloroanisole was prepared by the same procedure as described for Step 2 of Preparation 2a except using 2,4-dichloro-6-nitrophenol (52 g), methyl iodide (71 g), and potassium carbonate (41.4 g). Workup gave crude 2-nitro-4,6-dichloroanisole (50 g, 90%) which was used in the next step without purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06613786B2 |
| Source dataset | uspto-grants-2003_09 |
| ORD ID | ord-d012ac83f92c48888a9beb0d02d2ccbf |
| Source note | uspto-grants-2003_09 |