HuagongsheHuagongshe Chemistry Print Report · For research reference only
Stannous chloride dihydrate → (5-Chloro-4-methyl-2-methoxyphenyl)hydrazine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Stannous chloride dihydrate | HCID 61436 | — |
| Reactant | 5-Chloro-2-methoxy-4-methylaniline | HCID 22997628 | — |
| Reactant | Sodium Nitrite | HCID 23668193 | — |
| Product | (5-Chloro-4-methyl-2-methoxyphenyl)hydrazine | HCID 22997655 | 33.2% |
Reaction Steps
The title compound was prepared by the general procedure described above for Preparations 2a-i using 4-chloro-5-methyl-2-aminoanisole (10.26 g), NaNO2 (4.5 g), and SnCl2.2H2O (30 g). Workup gave 3.7 g (33%) of (5-chloro-4-methyl-2-methoxyphenyl)hydrazine.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06613786B2 |
| Source dataset | uspto-grants-2003_09 |
| ORD ID | ord-d393c0e6beba41adbc5d1fddef29b4bb |
| Source note | uspto-grants-2003_09 |