HuagongsheHuagongshe Chemistry Print Report · For research reference only
Azobisisobutyronitrile → Styrene glycidyl Methacrylate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Azobisisobutyronitrile | HCID 6547 | — |
| Reactant | Styrene | HCID 7501 | — |
| Reactant | Glycidyl methacrylate | HCID 7837 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | Styrene glycidyl Methacrylate | HCID 21867792 | — |
Reaction Steps
The same four-necked flask as used in Example 1 was charged with 100 g of toluene, and the temperature was adjusted to 80° C. with stirring under nitrogen. Then, 120 g of styrene, 89 g of glycidyl methacrylate and 0.1 g of azobisisobutyronitrile were added thereto and the reaction carried out in the same manner as in Example 1 to give a styrene-glycidyl methacrylate copolymer. This copolymer (96 weight parts) and 4 weight parts of 4,4′-bisazidobenzal(4-methyl)cyclohexanone were dissolved in 100 weight parts of xylene and the solution was subjected to polymerization in the same manner as in Example 1, whereupon an over coat film was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06613855B1 |
| Source dataset | uspto-grants-2003_09 |
| ORD ID | ord-a6513315a0884485aafab8d4df47f1db |
| Source note | uspto-grants-2003_09 |