3-Chloro-4-hydroxybenzohydrazide → 3-Chloro-4-hydroxybenzoic Acid 4-(3-Hydroxypropyl)naphthylmethylene Hydrazide

HRID 1166747Notes

Reaction equation

HRID 1166747 reaction equation
[CH:1]([C:3]1[C:12]2[C:7](=[CH:8][CH:9]=[CH:10][CH:11]=2)[C:6]([CH2:13][CH2:14][CH2:15][OH:16])=[CH:5][CH:4]=1)=O.[Cl:17][C:18]1[CH:19]=[C:20]([CH:25]=[CH:26][C:27]=1[OH:28])[C:21]([NH:23][NH2:24])=[O:22]>>[OH:16][CH2:15][CH2:14][CH2:13][C:6]1[C:7]2[C:12](=[CH:11][CH:10]=[CH:9][CH:8]=2)[C:3]([CH:1]=[N:24][NH:23][C:21](=[O:22])[C:20]2[CH:25]=[CH:26][C:27]([OH:28])=[C:18]([Cl:17])[CH:19]=2)=[CH:4][CH:5]=1

Participants

3

Reactant 2

HCID 109542683-Chloro-4-hydroxybenzohydrazideHCID 229990881-Formyl-4-(3-hydroxypropyl)naphthalene

Product 1

HCID 674836283-Chloro-4-hydroxybenzoic Acid 4-(3-Hydroxypropyl)naphthylmethylene Hydrazide

Procedure

This compound was prepared according to the general procedure for the synthesis of alkylidene hydrazones by condensation of 1-formyl-4-(3-hydroxypropyl) naphthalene from step B and 3-chloro-4-hydroxy benzoic acid hydrazide.

Workup

  1. customThis compound was prepared

Sources & evidence

ORD record
ord-f066b6540ff44906be2a1e6a5ec6173a
Source dataset
uspto-grants-2003_09
Patent number
US06613942B1

Reaction notes

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