Sodium Carbonate → HCID 72514303, compound

HRID 1166748Notes

Reaction equation

HRID 1166748 reaction equation
[CH:1]([C:3]1[C:12]2[C:7](=[CH:8][CH:9]=[CH:10][CH:11]=2)[C:6]([CH:13]=[CH:14][C:15]([O:17]CC)=[O:16])=[CH:5][CH:4]=1)=[O:2].C(=O)([O-])[O-].[Na+].[Na+]>O>[CH:1]([C:3]1[C:12]2[C:7](=[CH:8][CH:9]=[CH:10][CH:11]=2)[C:6]([CH:13]=[CH:14][C:15]([OH:17])=[O:16])=[CH:5][CH:4]=1)=[O:2]

Participants

4

Reactant 2

HCID 10340Sodium CarbonateHCID 131724059HCID 131724059, compound

Product 1

HCID 72514303HCID 72514303, compoundYield 94%

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Procedure

A suspension of ethyl 4-formylnaphthalene acrylate (391 mg, 1.53 mmol), sodium carbonate (195 mg, 1.84 mmol) in water (10 mL) was refluxed for 16 hr. The cold solution was filtered, and the filtrate was acidified with conc. hydrochloric acid. The precipitate was collected by suction and dried for 48 hr in vacuum to give the product (325 mg, 94%) as a yellow solid.

Workup

  1. temperaturewas refluxed for 16 hr
  2. filtrationThe cold solution was filtered
  3. customThe precipitate was collected by suction
  4. customdried for 48 hr in vacuum

Sources & evidence

ORD record
ord-4ef13b413ef345ee814108c054d94e8a
Source dataset
uspto-grants-2003_09
Patent number
US06613942B1

Reaction notes

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