3-Chloro-4-hydroxybenzohydrazide → HCID 70029087, compound
Reaction equation
[C:1]([O:5][C:6]1[C:15]2[C:10](=[CH:11][CH:12]=[CH:13][CH:14]=2)[C:9]([CH:16]=O)=[CH:8][CH:7]=1)(=[O:4])[CH:2]=[CH2:3].[Cl:18][C:19]1[CH:20]=[C:21]([CH:26]=[CH:27][C:28]=1[OH:29])[C:22]([NH:24][NH2:25])=[O:23]>>[C:1]([O:5][C:6]1[C:15]2[C:10](=[CH:11][CH:12]=[CH:13][CH:14]=2)[C:9]([CH:16]=[N:25][NH:24][C:22](=[O:23])[C:21]2[CH:26]=[CH:27][C:28]([OH:29])=[C:19]([Cl:18])[CH:20]=2)=[CH:8][CH:7]=1)(=[O:4])[CH:2]=[CH2:3]Participants
3
Procedure
The compound was prepared according to the general procedure for the synthesis of alkylidene hydrazones from the condensation of 4-formyl-1-naphthyl acrylate (from step C) and 3-chloro-4-hydroxy benzoic acid hydrazide.
Workup
- customThe compound was prepared
Sources & evidence
- ORD record
- ord-c89b247e2485401ab517e43c3ff363e2
- Source dataset
- uspto-grants-2003_09
- Patent number
- US06613942B1
Reaction notes
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