HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethylformamide → HCID 22998412, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethylformamide | HCID 6228 | — |
| Reactant | Sulfuryl chloride | HCID 24648 | — |
| Reactant | 2-Benzyl-1-benzothiophene | HCID 12758157 | — |
| Product | HCID 22998412 | HCID 22998412 | — |
Reaction Steps
2-Benzylbenzo[b]thiophene-3-sulfonyl chloride was prepared by the method of Example 40B with DMF (5.4 mmoles, 0.41 ml), sulfuryl chloride (4.6 mmoles, 0.37 ml) and 2-benzylbenzo[b]thiophene. Flash chromatography (5% ethyl acetate/hexanes) provided 0.55 g (64%) of a yellow solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06613804B2 |
| Source dataset | uspto-grants-2003_09 |
| ORD ID | ord-41c821e73ee04eccbe4bcd18c49d10f5 |
| Source note | uspto-grants-2003_09 |