HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Nitrophenyl isocyanate → HCID 15462733, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Nitrophenyl isocyanate | HCID 76835 | — |
| Reactant | 3-Methoxy-4-(oxazol-5-yl)aniline | HCID 15462732 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 15462733 | HCID 15462733 | 97% |
Reaction Steps
To a solution of 600 mg (3.2 mmol) of 1D in 20 ml of methylene chloride was added, as a solid, 525 mg (3.2 mmol) of m-nitrophenylisocyanate. A voluminous precipitate was obtained. Stirring was continued overnight. The precipitate was filtered and washed with methylene chloride to afford 1.1 g (3.1 mmol, 97%) of compound 17A as a yellow solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06617323B2 |
| Source dataset | uspto-grants-2003_09 |
| ORD ID | ord-16ad214397a74a9da7b19b12e1a55171 |
| Source note | uspto-grants-2003_09 |