HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,3-Dihydrobenzo(b)furan-5-carboxylic acid → HCID 12985421, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,3-Dihydrobenzo(b)furan-5-carboxylic acid | HCID 676583 | — |
| Reactant | 6,11-dihydro-5H-pyrido[2,3-b][1,5]benzodiazepine | HCID 11030760 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 12985421 | HCID 12985421 | — |
Reaction Steps
Prepared from 2,3-dihydro-benzofuran-5-carboxylic acid (0.328 g, 2 mmol) and 6,11-dihydro-5H-pyrido[2,3-b][1,5]benzodiazepine (0.398 g, 2 mmol) in a manner essentially identical to that of Example 1. The title compound was obtained as an off-white solid, m.p. 188° C., upon recrystallization from diethyl ether.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06620807B1 |
| Source dataset | uspto-grants-2003_09 |
| ORD ID | ord-7e0f7c5ba55f435f9ef9813b3924f07a |
| Source note | uspto-grants-2003_09 |