Cesium carbonate → HCID 10161511, compound

HRID 1167741Notes

Reaction equation

HRID 1167741 reaction equation
Br[C:2]1[CH:3]=[C:4]([CH:25]=[CH:26][N:27]=1)[C:5]([NH:7][C:8]1[S:9][C:10]2[C:16]([N:17]3[CH2:22][CH2:21][O:20][CH2:19][CH2:18]3)=[CH:15][CH:14]=[C:13]([O:23][CH3:24])[C:11]=2[N:12]=1)=[O:6].C(=O)([O-])[O-].[Cs+].[Cs+].[CH3:34][O:35][CH2:36][CH2:37][NH:38][CH3:39]>>[CH3:34][O:35][CH2:36][CH2:37][N:38]([CH3:39])[C:2]1[CH:3]=[C:4]([CH:25]=[CH:26][N:27]=1)[C:5]([NH:7][C:8]1[S:9][C:10]2[C:16]([N:17]3[CH2:18][CH2:19][O:20][CH2:21][CH2:22]3)=[CH:15][CH:14]=[C:13]([O:23][CH3:24])[C:11]=2[N:12]=1)=[O:6]

Participants

4

Reactant 3

HCID 10796Cesium carbonateHCID 300977(2-Methoxyethyl)(methyl)amineHCID 229934292-bromo-N-(4-methoxy-7-morpholin-4-yl-benzothiazol-2-yl)-isonicotinamide

Product 1

HCID 10161511HCID 10161511, compound

Procedure

From 2-bromo-N-(4-methoxy-7-mopholin-4-yl-benzothiazol-2-yl)-isonicotinamide with cesium carbonate and N-(2-methoxyethyl)-methylamine. ES-MS m/e (%): 458 (M+H+, 100).

Sources & evidence

ORD record
ord-5193a5a58f56406695e1b171599ae053
Source dataset
uspto-grants-2003_09
Patent number
US06620811B2

Reaction notes

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