HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Butanol → HCID 22993423, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Butanol | HCID 263 | — |
| Reactant | Sodium hydride | HCID 24758 | — |
| Reactant | HCID 22993400 | HCID 22993400 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 22993423 | HCID 22993423 | — |
Reaction Steps
From 6-chloro-N-(4-methoxy-7-mopholin-4-yl-benzothiazol-2-yl)-nicotinamide with sodium hydride and butanol in dioxane and DMF. ES-MS m/e (%): 465 (M+Na+, 40), 443 (M+H+, 100).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06620811B2 |
| Source dataset | uspto-grants-2003_09 |
| ORD ID | ord-aa874ce5010d4a19876f5546b1e9dc5d |
| Source note | uspto-grants-2003_09 |