HuagongsheHuagongshe Chemistry Print Report · For research reference only
(3R)-(+)-3-(Dimethylamino)pyrrolidine → HCID 69915777, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (3R)-(+)-3-(Dimethylamino)pyrrolidine | HCID 2758521 | — |
| Reactant | HCID 22994506 | HCID 22994506 | — |
| Product | HCID 69915777 | HCID 69915777 | 55% |
Reaction Steps
The product from Example 165C and (3R)-N,N-dimethyl-3-pyrrolidinamine were processed as described in Example 164D to provide the title compound (55% yield). 1HNMR (300 MHz, CDCl3) δ1.65 (m, 2H), 1.81 (bs, 2H), 2.00-2.85 (m, 15H), 3.0 (m, 1H), 4.13 (bs, 2H), 6.90-7.54 (m, 7H); MS (ESI) m/z 364 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06620839B2 |
| Source dataset | uspto-grants-2003_09 |
| ORD ID | ord-f7c6374e66c94845b63e9b62b954bd30 |
| Source note | uspto-grants-2003_09 |