HuagongsheHuagongshe Chemistry Print Report · For research reference only
(3R)-(+)-3-(Dimethylamino)pyrrolidine → HCID 69915980, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (3R)-(+)-3-(Dimethylamino)pyrrolidine | HCID 2758521 | — |
| Reactant | HCID 22994383 | HCID 22994383 | — |
| Product | HCID 69915980 | HCID 69915980 | 63% |
Reaction Steps
The product from Example 166C and (3R)-N,N-dimethyl-3-pyrrolidinamine were processed as described in Example 164D to provide the title compound (63% yield). 1HNMR (300 MHz, CDCl3) δ1.68 (m, 2H), 2.15 (m 4H), 2.23 (s, 6H), 2.30-2.95 (m, 5H), 4.15 (m, 2H), 7.00-7.63 (m, 7H); MS (ESI) m/z 368 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06620839B2 |
| Source dataset | uspto-grants-2003_09 |
| ORD ID | ord-a04899f19e9844b3837a298186a30212 |
| Source note | uspto-grants-2003_09 |