HuagongsheHuagongshe Chemistry Print Report · For research reference only
(3R)-(+)-3-(Dimethylamino)pyrrolidine → 461045-07-8
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (3R)-(+)-3-(Dimethylamino)pyrrolidine | HCID 2758521 | — |
| Reactant | HCID 22994370 | HCID 22994370 | — |
| Product | 461045-07-8 | HCID 9929160 | 60% |
Reaction Steps
The product from Example 167B and (3R)-N,N-dimethyl-3-pyrrolidinamine were processed as described in Example 164D to provide the title compound (60% yield). 1HNMR (300 MHz, CDCl3) δ2.00-3.00 (m, 16H), 3.20 (m, 1H), 4.20 (m, 2H), 7.10-7.75 (m, 7H); MS (ESI) m/z 368 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06620839B2 |
| Source dataset | uspto-grants-2003_09 |
| ORD ID | ord-55607f54e25c44d28decc42c4ac721f8 |
| Source note | uspto-grants-2003_09 |