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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1167863Generated: November 1, 2026

4-Bromo-m-cresol → HCID 22274489, compound

https://huagongshe.com/reaction/1167863

Reaction equation

Participants

RoleNameHCIDCharge
Reactant4-Bromo-m-cresolHCID 72857—
Reactant4-Cyanophenylboronic acidHCID 2734326—
ProductHCID 22274489HCID 2227448960%

Reaction Steps

4-Cyanophenylboronic acid and 4-bromo-3-methylphenol were processed as described in Example 167A to provide the title compound (60% yield). 1HNMR (300 MHz, CDCl3) δ2.20 (s, 3H), 4.68 (bs, 1H), 6.78 (m, 2H), 7.15 (m, 1H), 7.42 (m, 2H), 7.76(m, 2H); MS (CDI) m/z 227 (M+NH4)+.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06620839B2
Source datasetuspto-grants-2003_09
ORD IDord-4ec06e889cda45a899aa1d1b94cb7ebd
Source noteuspto-grants-2003_09