HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Bromo-m-cresol → HCID 22274489, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Bromo-m-cresol | HCID 72857 | — |
| Reactant | 4-Cyanophenylboronic acid | HCID 2734326 | — |
| Product | HCID 22274489 | HCID 22274489 | 60% |
Reaction Steps
4-Cyanophenylboronic acid and 4-bromo-3-methylphenol were processed as described in Example 167A to provide the title compound (60% yield). 1HNMR (300 MHz, CDCl3) δ2.20 (s, 3H), 4.68 (bs, 1H), 6.78 (m, 2H), 7.15 (m, 1H), 7.42 (m, 2H), 7.76(m, 2H); MS (CDI) m/z 227 (M+NH4)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06620839B2 |
| Source dataset | uspto-grants-2003_09 |
| ORD ID | ord-4ec06e889cda45a899aa1d1b94cb7ebd |
| Source note | uspto-grants-2003_09 |