Anisole → HCID 86585652, compound

Participants

Reaction Steps

Anisole (0.47 g, 4.28 mmol) and acetonitrile/dichloromethane (1/2, v/v, 25 ml) were added to t-butyl N-{2-[3-(9-acridinylamino)-5-(hydroxymethyl)anilino]-2-oxoethyl}carbamate (0.34 g, 0.71 mmol). To the resulting mixture, aluminium chloride (0.57 g, 4.28 mmol) was slowly added with stirring and stirred for 2 hours at the room temperature. The resulting product was concentrated under the reduced pressure and purified by column chromatography to give the titled compound.

Provenance & Evidence