HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 10120092, compound → HCID 10210262, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 10120092 | HCID 10120092 | — |
| Reactant | HCID 10209850 | HCID 10209850 | — |
| Product | HCID 10210262 | HCID 10210262 | — |
Reaction Steps
The title compound was prepared as a white foam in comparable yield according to the procedure described above for the preparation of N-[6-(acetyl-methyl-amino)-4-o-tolyl-pyridin-3-yl]-2-(3,5-bis-trifluoromethyl-phenyl)-N-methyl-isobutyramide using cyclopropanecarboxylic acid (5-{[2-(3,5-bis-trifluoromethyl-phenyl)-2-methyl-propionyl]-methyl-amino}-4-o-tolyl-pyridin-2-yl)-amide instead of N-(6-acetylamino-4-o-tolyl-pyridin-3-yl)-2-(3,5-bis-trifluoromethyl-phenyl)-N-methyl-isobutyramide. MS m/e (%): 600 (M+Na+, 22), 578 (M+H+, 100).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06624176B2 |
| Source dataset | uspto-grants-2003_09 |
| ORD ID | ord-055ea379ccca4a59880c74de34cc875f |
| Source note | uspto-grants-2003_09 |