HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzoyl chloride → HCID 9835841, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzoyl chloride | HCID 7412 | — |
| Reactant | Methyl 4-(4-aminophenyl)-4-oxobutanoate | HCID 12016833 | — |
| Product | HCID 9835841 | HCID 9835841 | 53.8% |
Reaction Steps
In a manner similar to that described in Example 3, benzoyl chloride (0.047 g, 0.00033 mol) was allowed to react with 4-(4-amino-phenyl)-4-oxo-butyric acid, methyl ester (0.052 g, 0.00025 mol), and the resulting intermediate was hydrolyzed to give 0.040 g of 4-[4-(benzoylamino)-phenyl]-4-oxo-butyric acid as an off-white solid; MS-(AP+) MH+332.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06624196B2 |
| Source dataset | uspto-grants-2003_09 |
| ORD ID | ord-96b7f50d2d1d470bbcaa2afc00981be1 |
| Source note | uspto-grants-2003_09 |