Dodecanoyl chloride → HCID 21361333, compound

Participants

Reaction Steps

In analogy to example 1 were reacted 6,36 g (2 mmol) of 2,6-diethyl-2,3,6-trimethyl-1-(1-phenyl-ethoxy)-piperidin-4-ol with 4,38 g (2 mmol) of lauroyl chloride and 2.02 g (2 mmol) of triethylamine in toluene to give 9,4 g (94%) dodecanoic acid 2,6-diethyl-2,3,6-trimethyl-1-(1-phenyl-ethoxy)-piperidin-4-yl ester as yellowish liquid. Elemental analysis calculated for C32H55NO3: C 76,59%; H 11,05%; N 2,79%. Found: C 76,17%; H 11,75%; N 2,69%.

Provenance & Evidence