HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzoyl chloride → N-Benzoyl-2'-O-(2-methoxyethyl)adenosine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzoyl chloride | HCID 7412 | — |
| Reactant | Tetrabutylammonium Fluoride | HCID 2724141 | — |
| Reactant | HCID 21348484 | HCID 21348484 | — |
| Product | N-Benzoyl-2'-O-(2-methoxyethyl)adenosine | HCID 21348490 | — |
Reaction Steps
5′-O-t-Butyldiphenylsilyl-2′-O-(methoxyethyl)adenosine is treated with TBAF as per the procedure of Example 8 and subsequently treated with benzoyl chloride as per the procedure of Example 4 to give the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06624294B2 |
| Source dataset | uspto-grants-2003_09 |
| ORD ID | ord-f966a965390c4ed9a4159614ea5b2f34 |
| Source note | uspto-grants-2003_09 |