化工社化工社 化学情報印刷レポート · 研究参考用
Sulfuric Acid → Sodium 3-hydroxypyrene-5-sulfonate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Sulfuric Acid | HCID 1118 | — |
| 反応物 | Pyranine | HCID 61388 | — |
| 生成物 | Sodium 3-hydroxypyrene-5-sulfonate | HCID 87551501 | 10% |
反応手順
Scheme 1 shows steps used to synthesize compound 3. Reaction of HPTS with 30% sulfuric acid at 150° C. for 20 min gave sodium 3-hydroxypyrene-5-sulfonate 1 in 10% yield. Acetylation of 1 followed by chlorination of 2 gave intermediate 3, which is analogous to our HPTS-Cl but with only one sulfonyl chloride.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07824918B2 |
| 出典データセット | uspto-grants-2010_11 |
| ORD ID | ord-d2ac55930bfd49cd8c31bca9633c57ff |
| 出典メモ | uspto-grants-2010_11 |