2-Methoxyethanol → HCID 58985622, compound

HRID 1169751Notes

Reaction equation

HRID 1169751 reaction equation
[Cl:1][C:2]1[N:7]=[C:6](Cl)[C:5](I)=[CH:4][N:3]=1.CC1(C)C(C)(C)OB([C:18]2[S:19][CH:20]=[CH:21][CH:22]=2)O1.[CH3:24][O:25][CH2:26][CH2:27][OH:28]>>[Cl:1][C:2]1[N:7]=[C:6]([O:28][CH2:27][CH2:26][O:25][CH3:24])[C:5]([C:20]2[S:19][CH:18]=[CH:22][CH:21]=2)=[CH:4][N:3]=1

Participants

4

Reactant 3

HCID 80192-MethoxyethanolHCID 2634382,4-Dichloro-5-iodopyrimidineHCID 107036284,4,5,5-Tetramethyl-2-(thiophen-2-yl)-1,3,2-dioxaborolane

Product 1

HCID 58985622HCID 58985622, compound

Procedure

Preparation according to procedures 4b and 3 with the use of 2,4-dichloro-5-iodopyrimidine, 2-methoxy-ethanol and 4,4,5,5-tetramethyl-2-(2-thienyl)-1,3,2-dioxaborolane.

Workup

  1. customPreparation

Sources & evidence

ORD record
ord-bb329590cf2b4b30877f66484ee908f1
Source dataset
uspto-grants-2010_11
Patent number
US07825128B2

Reaction notes

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