HRID1170010
反应详情
EQUATION
反应方程式
REACTANTS
反应物
PRODUCTS
生成物
CONDITIONS
反应条件
- 温度
- 150 °C
PROCEDURE
实验过程
3-[2-(Methoxycarbonyl)acetylamino]pyridine-4-carboxylic Acid (1.1 equivalents) was combined with 1,2-phenylenediamine (1.0 equivalent) and heated at 150° C. for 3 hours. The crude product was purified by reversed-phase HPLC (DMSO/5% TFA). LC/MS m/z 279.3 (MH+), Rt 1.73 minutes.
WORKUP
后处理
- customThe crude product was purified by reversed-phase HPLC (DMSO/5% TFA)