2-Methoxybenzylamine → HCID 24989335, compound

HRID 1170151Notes

Reaction equation

HRID 1170151 reaction equation
[N+:1]([C:4]1[CH:13]=[CH:12][CH:11]=[C:10]2[C:5]=1[CH:6]=[CH:7][C:8](Cl)=[N:9]2)([O-])=O.[CH3:15][O:16][C:17]1[CH:24]=[CH:23][CH:22]=[CH:21][C:18]=1[CH2:19][NH2:20].[CH3:25][C:26]1[NH:27][CH:28]=[C:29]([CH:31]=O)[N:30]=1>>[CH3:15][O:16][C:17]1[CH:24]=[CH:23][CH:22]=[CH:21][C:18]=1[CH2:19][NH:20][C:8]1[CH:7]=[CH:6][C:5]2[C:4]([NH:1][CH2:31][C:29]3[NH:30][C:26]([CH3:25])=[N:27][CH:28]=3)=[CH:13][CH:12]=[CH:11][C:10]=2[N:9]=1

Participants

4

Reactant 3

HCID 812922-MethoxybenzylamineHCID 3192512-Chloro-5-nitroquinolineHCID 178418999HCID 178418999, compound

Product 1

HCID 24989335HCID 24989335, compound

Procedure

The title compound, MS: m/e=374.4 (M+H+), was prepared from 5-nitro-2-chloroquinoline, 2-methoxybenzylamine and 2-methyl-1H-imidazole-4-carbaldehyde as described in example 26.

Sources & evidence

ORD record
ord-c09ae356673b4eeda54d19dc8c03a914
Source dataset
uspto-grants-2010_11
Patent number
US07825253B2

Reaction notes

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