1,3-Benzodioxole-4-carboxaldehyde → HCID 24989721, compound

HRID 1170156Notes

Reaction equation

HRID 1170156 reaction equation
[N+:1]([C:4]1[CH:13]=[CH:12][CH:11]=[C:10]2[C:5]=1[CH:6]=[CH:7][C:8](Cl)=[N:9]2)([O-])=O.[CH3:15][C:16]1[O:20][C:19]([CH2:21][NH2:22])=[CH:18][CH:17]=1.[CH2:23]1[O:33][C:32]2[C:25](=[C:26]([CH:29]=[CH:30][CH:31]=2)[CH:27]=O)[O:24]1>>[O:33]1[C:32]2[CH:31]=[CH:30][CH:29]=[C:26]([CH2:27][NH:1][C:4]3[C:5]4[CH:6]=[CH:7][C:8]([NH:22][CH2:21][C:19]5[O:20][C:16]([CH3:15])=[CH:17][CH:18]=5)=[N:9][C:10]=4[CH:11]=[CH:12][CH:13]=3)[C:25]=2[O:24][CH2:23]1

Participants

4

Reactant 3

HCID 822641,3-Benzodioxole-4-carboxaldehydeHCID 3192512-Chloro-5-nitroquinolineHCID 27246835-Methyl-2-furylmethylamine

Product 1

HCID 24989721HCID 24989721, compound

Procedure

The title compound, MS: m/e=388.4 (M+H+), was prepared from 5-nitro-2-chloroquinoline, 5-methyl-2-furanmethanamine and 2,3-(methylenedioxy)benzaldehyde as described in example 26.

Sources & evidence

ORD record
ord-93641addb75f4ec1a04ba75c1e9e6203
Source dataset
uspto-grants-2010_11
Patent number
US07825253B2

Reaction notes

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