Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
1-Phenyl-2-pyridin-2-ylethane-1,2-dione 2-oxime → 2-Amino-1-phenyl-2-pyridin-2-ylethanol
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 1-Phenyl-2-pyridin-2-ylethane-1,2-dione 2-oxime | HCID 136406848 | — |
| 반응물 | HCID 178418361 | HCID 178418361 | — |
| 촉매 | Platinum oxide (PtO) | HCID 82844 | — |
| 용매 | Ethanol | HCID 702 | — |
| 생성물 | 2-Amino-1-phenyl-2-pyridin-2-ylethanol | HCID 67524046 | — |
반응 단계
25.3 g of 1-phenyl-2-pyridin-2-ylethane-1,2-dione 2-oxime were dissolved in 300 ml of ethanol and, after addition of 1.0 g of platinum oxide, hydrogenated under atmospheric pressure until no further hydrogen was taken up. Filtration and concentration of the solution resulted in 21.6 g of 2-amino-1-phenyl-2-pyridin-2-ylethanol as mixture of 2 diastereomers.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07825264B2 |
| 출처 데이터셋 | uspto-grants-2010_11 |
| ORD ID | ord-a6abacd96d98429f9e5311bd0448a4f8 |
| 출처 메모 | uspto-grants-2010_11 |