HuagongsheHuagongshe Chemistry Print Report · For research reference only
Oxalyl chloride → HCID 86054523, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Oxalyl chloride | HCID 65578 | — |
| Reactant | 4-Iodo-2-propoxybenzenemethanol | HCID 68768450 | — |
| Solvent | Dimethyl Sulfoxide | HCID 679 | — |
| Product | HCID 86054523 | HCID 86054523 | — |
Reaction Steps
The procedure is the same as that described above, using 5.5 g, that is 18.8 mmol, of (4-iodo-2-propoxyphenyl)methanol, 1.8 ml of oxalyl chloride and 3 ml of DMSO. After evaporation of the solvents, 5.5 g (100%) of the expected compound are recovered in the form of a yellow solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07829588B2 |
| Source dataset | uspto-grants-2010_11 |
| ORD ID | ord-bdfa82decdb048e99081fb8e363156a0 |
| Source note | uspto-grants-2010_11 |