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HRID1171774

反应详情

EQUATION

反应方程式

HRID 1171774 的结构方程式

REACTANTS

反应物

2
结构：CCOC(=O)N=C=S
HCID85320

Ethyl isothiocyanatoformate

C4H5NO2S

结构：CCOC(=O)c1[nH]ccc1NCC(O[Si](C)(C)C(C)(C)C)c1ccc(OC)cc1
HCID67068499

未命名化合物

PRODUCTS

生成物

1
结构：COc1ccc(C(Cn2c(=S)[nH]c(=O)c3[nH]ccc32)O[Si](C)(C)C(C)(C)C)cc1
HCID86623128

未命名化合物

收率 90%

PROCEDURE

实验过程

The title compound (0.07 g, 90%) was prepared in accordance with general method B using 3-{[2-{[tert-butyl(dimethyl)silyl]oxy}-2-(4-methoxyphenyl)ethyl]amino}-1H-pyrrole-2-carboxylic acid ethyl ester (0.13 g, 0.31 mmol) and ethoxycarbonyl isothiocyanate (0.042 mL, 0.37 mmol).