HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dichloromethane → HCID 66853922, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dichloromethane | HCID 6344 | — |
| Reactant | HCID 58939869 | HCID 58939869 | — |
| Product | HCID 66853922 | HCID 66853922 | — |
Reaction Steps
To 0.30 g of tert-butyl 2-{[6-(9-oxoacridin-10(9H)-yl)hexanoyl]amino}ethylcarbamate was added dicholoromethane (DCM; 30 ml). HCl (g) was bubbled through the solution for 10 minutes. After this time the mixture was filtered and washed with DCM (3×20 ml) to give the desired product (0.15 g; Formula XIX). Mass spectrum: 352 (M+H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07829714B2 |
| Source dataset | uspto-grants-2010_11 |
| ORD ID | ord-71c067ae6bb34665bb794e88d77019a6 |
| Source note | uspto-grants-2010_11 |