Carbon Dioxide → HCID 178527662, compound

HRID 1172027Notes

Reaction equation

HRID 1172027 reaction equation
[CH2:1]([S:6]([OH:9])(=[O:8])=[O:7])[S:2]([OH:5])(=[O:4])=[O:3].C(=O)([O-])[O-].[Ag+2:14].C(=O)=O>O>[CH2:1]([S:6]([O-:9])(=[O:8])=[O:7])[S:2]([O-:5])(=[O:4])=[O:3].[Ag+2:14]

Participants

5

Reactant 3

HCID 280Carbon DioxideHCID 10427Methanedisulfonic acidHCID 178418647HCID 178418647, compound2×

Product 1

HCID 178527662HCID 178527662, compound

Reagents, catalysts & solvents 1

HCID 962WaterSolvent2×

Procedure

A 50% solution of methanedisulfonic acid in water (2.5 grams) was diluted in 25 mL of water into which, while stirring, silver carbonate (3.91 grams) was added slowly. The silver carbonate dissolved with effervescence of carbon dioxide. After the reaction was complete remaining insoluble material was removed by filtration and the filtrate was stripped of water and dried under high vacuum at 45° C. to give 4.9 grams of white crystals.

Workup

  1. customwas removed by filtration
  2. customdried under high vacuum at 45° C.

Sources & evidence

ORD record
ord-7bd1a6dd4a404260a7cdcc8cbba5a5f7
Source dataset
uspto-grants-2010_11
Patent number
US07833693B2

Reaction notes

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