HRID1172303

反应详情

EQUATION

反应方程式

HRID 1172303 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

A solution of 2-(3-Isopentyl-4-oxo-2-phenylthiazolidin-5-yl)acetic acid (2.2 g, 7.2 mmol) in EtOH (20 ml) and H2SO4 (1 ml) was refluxed for 16 hours. The solution was evaporated to dryness and the residue was taken up in EtOAc and washed with sat. aq. Na2CO3 (3×), brine and evaporated to give the desired product as an oil.

WORKUP

后处理

  1. customThe solution was evaporated to dryness
  2. washwashed with sat. aq. Na2CO3 (3×), brine
  3. customevaporated