HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Fluorobenzoyl chloride → HCID 3225919, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Fluorobenzoyl chloride | HCID 67879 | — |
| Reactant | HCID 47002965 | HCID 47002965 | — |
| Solvent | Dichloromethane methanol | HCID 21226129 | — |
| Product | HCID 3225919 | HCID 3225919 | 30% |
Reaction Steps
The compound was prepared following the procedure described in the Example 3(D), using 4-Fluoro-benzoyl chloride as the acyl chloride of choice and the 3-[3-(4-Fluoro-phenyl)-[1,2,4]oxadiazol-5-yl]-piperidine hydrochloride (already prepared before in the Example 4(B)). Yield: 30% (white powder); mp=82-83° C.; Rf=0.25 (DCM/MeOH: 98/2);
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07834035B2 |
| Source dataset | uspto-grants-2010_11 |
| ORD ID | ord-62261cf7f62b4e84950e5f9682794e90 |
| Source note | uspto-grants-2010_11 |