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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1172739Generated: October 30, 2026

3-Fluorobenzoyl chloride → HCID 3486255, compound

https://huagongshe.com/reaction/1172739

Reaction equation

Participants

RoleNameHCIDCharge
Reactant3-Fluorobenzoyl chlorideHCID 74376—
ReactantHCID 46737061HCID 46737061—
SolventDichloromethane methanolHCID 21226129—
ProductHCID 3486255HCID 348625553%

Reaction Steps

The compound was prepared following the procedure described in the Example 3(D), using 3-Fluoro-benzoyl chloride as the acyl chloride of choice and the 3-(3-Phenyl-[1,2,4]oxadiazol-5-yl)-piperidine hydrochloride (already prepared before in the Example 7). Yield: 53% (yellow oil); Rf=0.25 (DCM/MeOH: 98/2); LCMS (Tr): 4.77 min (Method C); MS (ES+) gave m/z: 352.3.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07834035B2
Source datasetuspto-grants-2010_11
ORD IDord-06cabd1c9b98478e9e706f61349dfcc9
Source noteuspto-grants-2010_11