Hydroxyamine hydrochloride → HCID 87541309, compound

Participants

Reaction Conditions

Reaction Steps

A mixture of the product from Step 3 (1.6 g, 4.0 mmol), hydroxylamine hydrochloride (2.8 g, 40 mmol) and sodium acetate (3.3 g, 40 mmol) in ethanol (40 mL) was stirred in a sealed tube at 60° C. for 48 h. The precipitate was filtered off and the filtrate was concentrated. The residue was purified by chromatography on silica gel to give the oxime product.

Provenance & Evidence