HuagongsheHuagongshe Chemistry Print Report · For research reference only
7-Aminoindole → HCID 178527228, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 7-Aminoindole | HCID 111634 | — |
| Reactant | 4-Sulfamoylbenzene-1-sulfonyl chloride | HCID 10956159 | — |
| Product | HCID 178527228 | HCID 178527228 | 69.4% |
Reaction Steps
767 mg (3.0 mmol) of 4-sulfamoylbenzenesulfonyl chloride was reacted with 264 mg (2.0 mmol) of 7-amino-1H-indole and treated, to give 445 mg of N-(1H-indole-7-yl)-4-sulfanoylbenzenesulfonamide. The resulting compound was chlorinated using N-chlorosuccinimide in dichloromethane, to give 349 mg of the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07834049B2 |
| Source dataset | uspto-grants-2010_11 |
| ORD ID | ord-d24f49b68bf944d79c2e8a820fc732a0 |
| Source note | uspto-grants-2010_11 |