HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trifluoroacetic acid methylene chloride → Trifluoroacetic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trifluoroacetic acid methylene chloride | HCID 21863450 | — |
| Reactant | HCID 57717460 | HCID 57717460 | — |
| Product | Trifluoroacetic acid | HCID 6422 | — |
| Product | HCID 57717460 | HCID 57717460 | — |
Reaction Steps
A solution of N-(2-aminophenyl)-6-(3,9-diazaspiro[5.5]undec-3-yl)nicotinamide (10 mg, 0.022 mmol) in 2 mL of 1:1 TFA/CH2Cl2 was stirred for 1 h and concentrated, giving the title compound as a TFA salt; MS (ESI+): cal'd [M+1]+ 365.2, obs'd 365.2.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07834026B2 |
| Source dataset | uspto-grants-2010_11 |
| ORD ID | ord-8ab1fb96462a49b3acf0892c8fb6e457 |
| Source note | uspto-grants-2010_11 |