HuagongsheHuagongshe Chemistry Print Report · For research reference only
tert-butyl [(3R)-1-(cis-2-azidocyclohexyl)pyrrolidin-3-yl]carbamate → HCID 86608974, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | tert-butyl [(3R)-1-(cis-2-azidocyclohexyl)pyrrolidin-3-yl]carbamate | HCID 86608975 | — |
| Solvent | 1,4-Dioxane hydrochloride | HCID 20443148 | — |
| Product | HCID 86608974 | HCID 86608974 | 124.5% |
Reaction Steps
The mixture of tert-butyl [(3R) -1-(cis-2-azidocyclohexyl)pyrrolidin-3-yl]carbamate (0.57 g, 1.842 mmol) in 4 N HCl/dioxane (10 mL) was stirred at room temperature for 1 hour. The solution was concentrated to give 0.48 g of the title compound as HCl salt. MS (EI) calcd: (M+H)+=210.2; found: 210.2.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07834021B2 |
| Source dataset | uspto-grants-2010_11 |
| ORD ID | ord-a7e2dd42bce841a387ac84e0cbe9d928 |
| Source note | uspto-grants-2010_11 |