Aluminium lithium hydride → HCID 10062075, compound

HRID 1173306Notes

Reaction equation

HRID 1173306 reaction equation
C([O:5][C:6]1[CH:11]=[C:10]([C:12]([CH3:15])([CH3:14])[CH3:13])[CH:9]=[C:8]([C:16]([CH3:19])([CH3:18])[CH3:17])[C:7]=1[CH2:20][NH:21][C:22](=O)[CH2:23][CH3:24])(=O)CC.[H-].[Al+3].[Li+].[H-].[H-].[H-]>>[C:16]([C:8]1[C:7]([CH2:20][NH:21][CH2:22][CH2:23][CH3:24])=[C:6]([OH:5])[CH:11]=[C:10]([C:12]([CH3:14])([CH3:13])[CH3:15])[CH:9]=1)([CH3:17])([CH3:18])[CH3:19]

Participants

3

Reactant 2

HCID 21226445Aluminium lithium hydrideHCID 68718110HCID 68718110, compound

Product 1

HCID 10062075HCID 10062075, compound

Procedure

Using the procedure described in Example 20, the product of Step A from was reduced with lithium aluminum hydride to afford the title compound.

Sources & evidence

ORD record
ord-bedbc90b994c4b399f61ab23413b7e2b
Source dataset
uspto-grants-2010_11
Patent number
US07834062B2

Reaction notes

Loading…