4-Methoxyphenol → HCID 11653986, compound

HRID 1173387Notes

Reaction equation

HRID 1173387 reaction equation
[CH:1]1([CH2:4][N:5]([CH2:18][CH2:19][OH:20])[C:6]2[CH:13]=[CH:12][C:9]([C:10]#[N:11])=[C:8]([C:14]([F:17])([F:16])[F:15])[CH:7]=2)[CH2:3][CH2:2]1.[CH3:21][O:22][C:23]1[CH:28]=[CH:27][C:26](O)=[CH:25][CH:24]=1>>[CH:1]1([CH2:4][N:5]([CH2:18][CH2:19][O:20][C:26]2[CH:27]=[CH:28][C:23]([O:22][CH3:21])=[CH:24][CH:25]=2)[C:6]2[CH:13]=[CH:12][C:9]([C:10]#[N:11])=[C:8]([C:14]([F:16])([F:17])[F:15])[CH:7]=2)[CH2:2][CH2:3]1

Participants

3

Reactant 2

HCID 90154-MethoxyphenolHCID 11369616HCID 11369616, compound

Product 1

HCID 11653986HCID 11653986, compound

Procedure

Synthesized as described in Example 1C from 4-[(cyclopropylmethyl)(2-hydroxyethyl)amino]-2-(trifluoromethyl)benzonitrile and 4-methoxyphenol: MS (APCI) m/z 391 (M+1).

Workup

  1. customSynthesized

Sources & evidence

ORD record
ord-a91ee3c66fc945418ddb3cf05398d19e
Source dataset
uspto-grants-2010_11
Patent number
US07834063B2

Reaction notes

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