p-Hydroxybenzenesulfonamide → HCID 11641070, compound

HRID 1173462Notes

Reaction equation

[CH3:1][C:2]([CH3:21])([CH3:20])[CH2:3][N:4]([CH2:17][CH2:18][OH:19])[C:5]1[CH:12]=[CH:11][C:8]([C:9]#[N:10])=[C:7]([C:13]([F:16])([F:15])[F:14])[CH:6]=1.O[C:23]1[CH:28]=[CH:27][C:26]([S:29]([NH2:32])(=[O:31])=[O:30])=[CH:25][CH:24]=1>>[C:9]([C:8]1[CH:11]=[CH:12][C:5]([N:4]([CH2:3][C:2]([CH3:21])([CH3:20])[CH3:1])[CH2:17][CH2:18][O:19][C:23]2[CH:28]=[CH:27][C:26]([S:29]([NH2:32])(=[O:31])=[O:30])=[CH:25][CH:24]=2)=[CH:6][C:7]=1[C:13]([F:14])([F:15])[F:16])#[N:10]

Participants

Reactant 2

HCID 74093p-Hydroxybenzenesulfonamide

HCID 68495138HCID 68495138, compound

Product 1

HCID 11641070HCID 11641070, compound

Procedure

Synthesized as described in Example 1C from 4-[(2,2-dimethylpropyl)(2-hydroxyethyl)amino]-2-(trifluoromethyl)benzonitrile and 4-hydroxybenzenesulfonamide: MS (APCI) m/z 454 (M−1).

Workup

customSynthesized

Sources & evidence

ORD record: ord-a80b44eb34db46ae996989538ab1d70b
Source dataset: uspto-grants-2010_11
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US07834063B2

Reaction notes

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