HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 59556943, compound → HCID 67105280, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 59556943 | HCID 59556943 | — |
| Reactant | L-SELECTRIDE tetrahydrofuran | HCID 131725857 | — |
| Product | HCID 67105280 | HCID 67105280 | — |
Reaction Steps
Using 2-chloro-4-[5-(hydroxymethyl)-3,3-dimethyl-2,4-dioxopyrrolidin-1-yl]benzonitrile (80 mg) and lithium tri(sec-butyl)borohydride-THF solution (0.82 mL, 1 mol/L), and in the same manner as in Example 5, the title compound was obtained as colorless crystals (yield: 45.4 mg, 56%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07834051B2 |
| Source dataset | uspto-grants-2010_11 |
| ORD ID | ord-9622c9ee44d54667b1daaf27a22559d8 |
| Source note | uspto-grants-2010_11 |