HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanol → HCID 178419029, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanol | HCID 887 | — |
| Reactant | Sodium Methoxide | HCID 10942334 | — |
| Reactant | HCID 178418385 | HCID 178418385 | — |
| Product | HCID 178419029 | HCID 178419029 | 97% |
Reaction Steps
g (0.25 mol) of benzotriazole were reacted with an equivalent amount of methanolic sodium methoxide solution in 200 ml of methanol by the process described for catalyst 1. The reaction mixture was worked up as described above to give 34.2 g of sodium benzotriazolate (yield: 97% of theory) in the form of a virtually colourless powder. The product was pure according to its 1H-NMR spectrum and free from starting material.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07098289B2 |
| Source dataset | uspto-grants-2006_08 |
| ORD ID | ord-85c4cc847f3b41818b67922d54cd55aa |
| Source note | uspto-grants-2006_08 |