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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1174312Generated: November 2, 2026

Hydrochloric Acid → HCID 67407217, compound

https://huagongshe.com/reaction/1174312

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHydrochloric AcidHCID 313—
ReactantHCID 86726225HCID 86726225—
CatalystPalladiumHCID 23938—
SolventMethanolHCID 887—
ProductHCID 67407217HCID 67407217—

Reaction Conditions

Temperature25 °C

Reaction Steps

A solution containing the product from Example 113E (0.049 mmol) in methanol (1 mL) was treated with Pd on carbon (0.005 g, 10% Pd by wt.) and HCl solution (0.050 ML, 4N in dioxane), stirred under a hydrogen atmosphere (balloon pressure) at 25° C. for 16 hours, filtered through a bed of celite®, rinsed with methanol, and concentrated to give the title compound as the hydrochloride salt.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07834043B2
Source datasetuspto-grants-2010_11
ORD IDord-3a4ce4a231ab4be8bf3bf9e7926f7206
Source noteuspto-grants-2010_11