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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1174313Generated: October 28, 2026

Hydrochloric Acid → HCID 67408610, compound

https://huagongshe.com/reaction/1174313

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHydrochloric AcidHCID 313—
ReactantHCID 86726226HCID 86726226—
CatalystPalladiumHCID 23938—
SolventMethanolHCID 887—
ProductHCID 67408610HCID 67408610—

Reaction Conditions

Temperature25 °C

Reaction Steps

A solution containing the product from Example 114A (0.049 mmol) in methanol (1 mL) was treated with Pd on carbon (0.005 g, 10% Pd by wt.) and HCl solution (0.050 mL, 4N in dioxane), stirred under a hydrogen atmosphere (balloon pressure) at 25° C. for 3 hours, filtered through a bed of celite®, rinsed with methanol, and concentrated to give the title compound as the hydrochloride salt.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07834043B2
Source datasetuspto-grants-2010_11
ORD IDord-b6397f8392444dca873a2a0444b8f923
Source noteuspto-grants-2010_11