Trifluoroacetic acid → HCID 67406613, compound

Participants

Reaction Conditions

Reaction Steps

A solution containing the product from Example 132A (0.017 g, 0.023 mmol) in dichloromethane (1 mL) was added trifluoroacetic acid (1 mL), and the mixture was stirred at 25° C. for 1 hour, and concentrated. The residue was partitioned between ethyl acetate and saturated NaHCO3, and the organic phase was washed with brine and dried over MgSO4, filtered and concentrated to give the product, which was used without further purification.

Provenance & Evidence